Thermal Methods of Analysis

Thermal Methods of Analysis PDF Author: Wesley William Wendlandt
Publisher: Wiley-Interscience
ISBN:
Category : Thermal analysis
Languages : en
Pages : 536

Book Description


Thermal Methods of Analysis

Thermal Methods of Analysis PDF Author: P.J. Haines
Publisher: Springer Science & Business Media
ISBN: 9401113246
Category : Science
Languages : en
Pages : 297

Book Description
The wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu tors by colleagues and instrument manufacturers is most gratefully ack nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC).

Calorimetry and Thermal Methods in Catalysis

Calorimetry and Thermal Methods in Catalysis PDF Author: Aline Auroux
Publisher: Springer Science & Business Media
ISBN: 3642119549
Category : Technology & Engineering
Languages : en
Pages : 561

Book Description
The book is about calorimetry and thermal analysis methods, alone or linked to other techniques, as applied to the characterization of catalysts, supports and adsorbents, and to the study of catalytic reactions in various domains: air and wastewater treatment, clean and renewable energies, refining of hydrocarbons, green chemistry, hydrogen production and storage. The book is intended to fill the gap between the basic thermodynamic and kinetics concepts acquired by students during their academic formation, and the use of experimental techniques such as thermal analysis and calorimetry to answer practical questions. Moreover, it supplies insights into the various thermal and calorimetric methods which can be employed in studies aimed at characterizing the physico-chemical properties of solid adsorbents, supports and catalysts, and the processes related to the adsorption desorption phenomena of the reactants and/or products of catalytic reactions. The book also covers the basic concepts for physico-chemical comprehension of the relevant phenomena. Thermodynamic and kinetic aspects of the catalytic reactions can be fruitfully investigated by means of thermal analysis and calorimetric methods, in order to better understand the sequence of the elemental steps in the catalysed reaction. So the fundamental theory behind the various thermal analysis and calorimetric techniques and methods also are illustrated.

The Nature of Biological Systems as Revealed by Thermal Methods

The Nature of Biological Systems as Revealed by Thermal Methods PDF Author: Dénes Lörinczy
Publisher: Springer Science & Business Media
ISBN: 1402022190
Category : Science
Languages : en
Pages : 358

Book Description
Af ter a kind mo ti va tion by Judit Si mon (Ed i tor-in-Chief of the Jour nal of Ther mal Anal y s is and Cal o ri m e t r y, Kluwe r Ac a dem ic Pub lis her) and ne go ti a tions with po- si ble con tri bu tors - lasting for m ore than one year - it was de cided to write a book about the ap pli ca tion of ther mal meth ods in bi ol ogy. Its aim was to be a guide how to per form ex per i ments and what kind of in for mation m ight be gained by them. We tried to col lect in for mation tha t could be achieved only dur ing a long per sonal pra- tice. In this way sci en tists from bi ol ogy and med i cine, e. g., who are not so skilled in phys ics and math e mat ics may re al ize very soon the beauty and power of this tool at one hand. On the other hand, those sci en tists with better back ground in nat u ral sc- ences can be more sensitive to find out exciting biological problems.

Thermal Methods of Polymer Analysis

Thermal Methods of Polymer Analysis PDF Author: T.R Crompton
Publisher: Smithers Rapra
ISBN: 184735663X
Category : Science
Languages : en
Pages : 256

Book Description
This book reviews the various thermal methods used for the characterisation of polymer properties and composition. All these methods study the properties of polymers as they change with temperature. The methods discussed in this book are: differential photocalorimetry, differential scanning calorimetry, dielectric thermal analysis, differential thermal analysis, dynamic mechanical analysis, evolved gas analysis, gas chromatography, gas chromatography combined with mass spectrometry, mass spectrometry, microthermal analysis, thermal volatilisation, thermogravimetric analysis and thermomechanical analysis. Each technique is discussed in detail and examples of the use of each technique are also given. Each chapter has an extensive list of references so that the reader can follow up topics of interest. This book will be a useful reference for those who already use any of these thermal methods but will also be of interest to undergraduates and those who are just starting to use these techniques.

Electro-thermal Methods of Iron and Steel Production

Electro-thermal Methods of Iron and Steel Production PDF Author: John Baker Cannington Kershaw
Publisher:
ISBN:
Category : Electrometallurgy
Languages : en
Pages : 272

Book Description


Advanced Analytic and Control Techniques for Thermal Systems with Heat Exchangers

Advanced Analytic and Control Techniques for Thermal Systems with Heat Exchangers PDF Author: Libor Pekar
Publisher: Academic Press
ISBN: 0128194235
Category : Science
Languages : en
Pages : 522

Book Description
Advanced Analytic Control Techniques for Thermal Systems with Heat Exchangers presents the latest research on sophisticated analytic and control techniques specific for Heat Exchangers (HXs) and heat Exchanger Networks (HXNs), such as Stability Analysis, Efficiency of HXs, Fouling Effect, Delay Phenomenon, Robust Control, Algebraic Control, Geometric Control, Optimal Control, Fuzzy Control and Artificial Intelligence techniques. Editor Libor Pekar and his team of global expert contributors combine their knowledge and experience of investigated and applied systems and processes in this thorough review of the most advanced networks, analyzing their dynamics, efficiency, transient features, physical properties, performance, feasibility, flexibility and controllability. The structural and dynamic analyses and control approaches of HXNs, as well as energy efficient manipulation techniques are discussed, in addition to the design of the control systems through the full life cycle. This equips the reader with an understanding of the relevant theory in a variety of settings and scenarios and the confidence to apply that knowledge to solve problems in an academic or professional setting.Graduate students and early-mid career professionals require a robust understanding of how to suitably design thermal systems with HXs and HXNs to achieve required performance levels, which this book offers in one consolidated reference. All examples and solved problems included have been tried and tested, and these combined with the research driven theory provides professionals, researchers and students with the most recent techniques to maximize the energy efficiency and sustainability of existing and new thermal power systems. Analyses several advanced techniques, the theoretical background of these techniques and includes models, examples and results throughout Focusses on advanced analytic and control techniques which have been investigated or applied to thermal systems with HXs and HXNs Includes practical applications and advanced ideas from leading experts in the field, as well as case studies and tested problems and solutions

Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry PDF Author:
Publisher: Elsevier
ISBN: 0444640630
Category : Science
Languages : en
Pages : 860

Book Description
Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications

Principles of Thermal Analysis and Calorimetry

Principles of Thermal Analysis and Calorimetry PDF Author: Simon Gaisford
Publisher: Royal Society of Chemistry
ISBN: 1788018133
Category : Science
Languages : en
Pages : 280

Book Description
The use of thermal and calorimetric methods has shown rapid growth over the past few decades, in an increasingly wide range of applications. The original text was published in 2001; since then there have been significant advances in various analytical techniques and their applications. This second edition supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Written by experts in their field, brief accounts of the basic theory are reinforced with detailed technical advances and contemporary developments. Where appropriate, applications are used to highlight particular operating principles or methods of interpretation. As an important source of information for many levels of readership in a variety of areas, this book will be an aid for students and lecturers through to industrial and laboratory staff and consultants.

THERMAL METHODS (SET PRICE OF 34 BOOKS)

THERMAL METHODS (SET PRICE OF 34 BOOKS) PDF Author: James W. Dodd
Publisher: John Wiley & Sons
ISBN: 9788126517398
Category :
Languages : en
Pages : 364

Book Description
This flexible, self-contained tutorial outlines basic thermal methods, their extremely wide range of application, and the ways in which they are affected by experimental conditions. Numerous exercises are designed to bridge the gap between theory and practice, and self-assessment questions and interpretive exercises using real, raw laboratory data provide students with a practical, overall grasp of the subject which can then be followed up with more detailed readings suggested in the bibliography. By the end of this tutorial, students will know how to set up, calibrate, and operate a thermobalance calorimeter (for DSC) or analyser (for DTA); select optimimum operating conditions for obtaining thermal data by TG/DSC/DTA; prepare a variety of samples for thermal analysis and many other basic techniques. The ``open learning'' approach allows students to work on their own at their own pace.