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Author: G. C. Ulmer Publisher: Springer Science & Business Media ISBN: 3642880975 Category : Science Languages : en Pages : 368
Book Description
Within the last two decades, the experimental technology for the study of high temperature solid-vapor and liquid-vapor equilibria has mushroomed so fast that· both academic and industrial research ers desirous of working in this field -- be they physical chemists, metallurgists, ceramists, petrologists, crystal chemists, or mem bers of any of the several branches of materials science -- find themselves in the situation that in order to learn the art of the latest techniques, a period of apprenticeship or residency needs be spent at an institution or laboratory currently engaged in this type of solid-vapor or liquid-vapor research. The tech niques for control of the vapor phase at total pressures of one atmosphere or greater have not been well defined in the literature. Therefore, the purpose of this volume will be to serve as a labora tory manual for the control, calibration, and measurement of high temperature-high pressure equilibria. The avowed aims of this treatment of experimental techniques are: (1) to give, in terms understandable at the graduate student level, the laboratory procedures necessary to the design and utilization of good experimental technique, (2) to list the limitations, dangers, and technical pitfalls inherent or intrinsic to the described techniques, (3) to give theory and specific data only where they are essential to the experimental design, (4) to give with each chapter references that are extensive enough to serve as a bibliography of the state-of-the-art of technique development within the last decade.
Author: G. C. Ulmer Publisher: Springer Science & Business Media ISBN: 3642880975 Category : Science Languages : en Pages : 368
Book Description
Within the last two decades, the experimental technology for the study of high temperature solid-vapor and liquid-vapor equilibria has mushroomed so fast that· both academic and industrial research ers desirous of working in this field -- be they physical chemists, metallurgists, ceramists, petrologists, crystal chemists, or mem bers of any of the several branches of materials science -- find themselves in the situation that in order to learn the art of the latest techniques, a period of apprenticeship or residency needs be spent at an institution or laboratory currently engaged in this type of solid-vapor or liquid-vapor research. The tech niques for control of the vapor phase at total pressures of one atmosphere or greater have not been well defined in the literature. Therefore, the purpose of this volume will be to serve as a labora tory manual for the control, calibration, and measurement of high temperature-high pressure equilibria. The avowed aims of this treatment of experimental techniques are: (1) to give, in terms understandable at the graduate student level, the laboratory procedures necessary to the design and utilization of good experimental technique, (2) to list the limitations, dangers, and technical pitfalls inherent or intrinsic to the described techniques, (3) to give theory and specific data only where they are essential to the experimental design, (4) to give with each chapter references that are extensive enough to serve as a bibliography of the state-of-the-art of technique development within the last decade.
Author: Robert M. Hazen Publisher: Walter de Gruyter GmbH & Co KG ISBN: 1501508709 Category : Science Languages : en Pages : 604
Book Description
Volume 41 of Reviews in Mineralogy and Geochemistry introduces to the field of high-temperature and high-pressure crystal chemistry, both as a guide to the dramatically improved techniques and as a summary of the voluminous crystal chemical literature on minerals at high temperature and pressure. The three parts of the book introduces crystal chemical considerations of special relevance to non-ambient crystallographic studies, reviews the temperature- and pressure-variation of structures in major mineral groups and presents experimental techniques for high-temperature and high-pressure studies of single crystals and polycrystalline samples as well as special considerations relating to diffractometry on samples at non-ambient conditions.
Author: W. F. Sherman Publisher: ISBN: Category : Science Languages : en Pages : 496
Book Description
This book is divided into two sections - the first dealing with the components that work up the high pressure system and the second with the experiments that may be performed with high pressure equipment of relevance to a wide range of disciplines.
Author: John S. Waugh Publisher: Academic Press ISBN: 148328154X Category : Science Languages : en Pages : 324
Book Description
Advances in Magnetic Resonance, Volume 6 focuses on the theoretical and practical aspects of applying magnetic resonance methods to various problems in physical chemistry, emphasizing the different aspects of the exegesis of these problems. This book discusses the gas phase magnetic resonance of electronically excited molecules; techniques for observing excited electronic states; NMR studies in liquids at high pressure; and effect of pressure on self-diffusion in liquids. The nuclear magnetic resonance investigations of organic free radicals; measurement of proton coupling constants by NMR; and crystal point group symmetry and microscopic tensor properties in magnetic resonance spectroscopy are also elaborated. This text likewise deliberates the degeneracy of symmetry-related tensors; second and fourth moments in NQR spectroscopy for spins with I = 1; and fourth moment for equivalent nuclei with spins I = 1. This publication is valuable to physical chemists and students aiming to acquire knowledge on the application of magnetic resonance methods.
Author: Rudolf A. Steinbrecht Publisher: Springer Science & Business Media ISBN: 3642728154 Category : Science Languages : en Pages : 308
Book Description
To preserve tissue by freezing is an ancient concept going back pre sumably to the practice of ice-age hunters. At first glance, it seems as simple as it is attractive: the dynamics of life are frozen in, nothing is added and nothing withdrawn except thermal energy. Thus, the result should be more life-like than after poisoning, tan ning and drying a living cell as we may rudely call the conventional preparation of specimens for electron microscopy. Countless mishaps, however, have taught electron microscopists that cryotechniques too are neither simple nor necessarily more life-like in their outcome. Not too long ago, experts in cryotechniques strictly denied that a cell could truly be vitrified, i.e. that all the solutes and macro molecules could be fixed within non-crystalline, glass-like solid water without the dramatic shifts and segregation effects caused by crystallization. We now know that vitrification is indeed pos sible. Growing insight into the fundamentals of the physics of water and ice, as well as increasing experience of how to cool cells rapidly enough have enlivened the interest in cryofixation and pro duced a wealth of successful applications.
Author: G. C. Ulmer
Author: G. C. Ulmer
Author: G C Ulmer
Author: Robert M. Hazen
Author: W. F. Sherman
Author: S. A. Kulin
Author: John S. Waugh
Author: Hans D. Hochheimer
Author: 
Author: Rudolf A. Steinbrecht
Author: